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Ohio State University Campus Chemical Instrument Center NMR Core Facility

The Ohio State University

Contact Info:

Alex Hansen

151 W Woodruff Ave

Columbus, OH 43210

https://ccic.osu.edu/nmr

Grants and Identifiers:

RRID: RRID:SCR_027162

Instrumentation:

(Equipment No Longer Active At this Facility)

Andor iXon Ultra EMCCD camera

Scientific camera with EMCCD image sensor that is capable of detecting single photon events without image intensifier, achievable by way of unique electron multiplying structure built into the chip. [Product Link]

RRID:SCR_023166

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(Equipment No Longer Active At this Facility)

Bruker Avance NMR Spectrometer

Bruker’s Avance NMR spectrometers are utilized in various scientific fields to elucidate the structure, dynamics, and interactions of molecules. Avance spectrometers are composed of three main hardware components: console, which is the central control unit of the NMR spectrometer, and houses sophisticated electronics for the generation of the pulse sequences and for data acquisition and processing; superconducting magnet to generate homogenous and stable magnetic field to polarize the nuclear spins in the sample; probe for transmitting radiofrequency pulses and detecting the resulting signals from the sample. [Product Link]

RRID:SCR_027378

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Bruker: Avance III HD Ascend 850 MHz NMR Spectrometer

High-field nuclear magnetic resonance (NMR) spectrometer manufactured by Bruker Corporation with Console Brand: Avance III HD, Magnet Brand: Ascend and Field Strength: 850 MHz. Equipped with a cryo-cooled probe that cools the electronics with liquid helium or nitrogen to reduce thermal noise and boost signal sensitivity. Software: TopSpin 3.7 running on CentOS 7; Probe: 5mm Triple-resonance Inverse (TCI) cryoprobe with Z-Gradients; Features: Temperature controlled SampleCase (up to 24 samples), Nitrogen Liquefier, Dual-Receiver, High-sensitivity 1H & 13C. Used in structural biology, chemistry, and materials science to determine the molecular structure, dynamics, and interactions of complex molecules. [Product Link]

RRID:SCR_028484

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Bruker 1200 MHz NMR Spectrometer

(Equipment No Longer Active At this Facility)

Bruker 1200 MHz NMR Spectrometer (Liberty)

The nation’s only 1.2 GHz MHz equipped with a broad range of solution and solid-state probes

Bruker 600 MHz DNP-NMR Spectrometer (Skye)

CCIC’s 600 MHz NMR equipped with solid-state DNP probes.

Bruker 600 MHz NMR Spectrometer (Rubble)

CCIC’s 600 MHz NMR equipped with high sensitivity HCN cryoprobe.

Bruker 600 MHz NMR Spectrometer (Sage)

CCIC’s 600 MHz NMR equipped with broadband iProbe.

Bruker 700 MHz NMR Spectrometer (Rocky)

CCIC’s 700 MHz NMR equipped with high sensitivity 13C cryoprobe.

Bruker 800 MHz NMR Spectrometer (Everest)

CCIC’s 800 MHz wide-bore NMR equipped with ultrafast spinning MAS solid-state probes and more.

Bruker 800 MHz NMR Spectrometer (Ryder)

CCIC's 800 MHz NMR equipped with HCNP quad-channel cryoprobe.

Bruker 800 MHz NMR Spectrometer (Zuma)

CCIC’s 800 MHz narrow-bore NMR equipped with ultrafast spinning MAS solid-state probes, HR-MAS, and more.

(Equipment No Longer Active At this Facility)

Bruker 850 MHz NMR Spectrometer

CCIC's 850 MHz NMR equipped with high sensitivity HCN-Cryoprobe. Ideal for metabolomics, natural products, and biomolecular research.

(Equipment No Longer Active At this Facility)

Bruker 850 MHz NMR Spectrometer (Marshall)

CCIC's 850 MHz NMR equipped with high sensitivity HCN cryoprobe.

Services Provided:

Consultation

Data Analysis

DOSY NMR

Experimental Design

High And Low Temperature NMR

Macromolecule NMR

NMR Instrument Access

Nuclear Magnetic Resonance (NMR)

Polymer NMR

Protein NMR

Qualitative And Quantitative NMR Analysis

Sample Preparation

Small Molecule NMR

Solid State NMR

Training

Relevant Publications:

Description:

Advanced high-field NMR facility combines many capabilities spanning solution and solid state NMR, high sensitivity cryoprobes, ultrafast spinning MAS probes, as well as Dynamic Nuclear Polarization.